%0 Journal Article %@holdercode {isadg {BR SPINPE} ibi 8JMKD3MGPCW/3DT298S} %@nexthigherunit 8JMKD3MGPCW/3ESR3H2 %@archivingpolicy denypublisher denyfinaldraft24 %@usergroup administrator %@usergroup banon %@usergroup simone %3 two step.pdf %B Vacuum %X This paper reports the results of a two-step hot filament chemical vapor deposition method to improve the quality of diamond films. Diamond films were deposited on a Si(100) substrate having an area of 45 cm(2) and a thickness of 60 mu m. employing a HFCVD system. The first step is the growth of CVD diamond in the HFCVD reactor. In the second step, the samples were treated in a saturated solution of H2SO4:CrO3 and rinsed in a (1:1) solution of H2O2: NH4OH. After this procedure, a second diamond layer was deposited. The diamond films were analyzed by raman scattering spectroscopy (RSS). scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy (XPS). The films showed a high degree of purity with a thickness of 60 mu m, presenting uniform characteristics over a large area. %@mirrorrepository sid.inpe.br/mtc-m18@80/2008/03.17.15.17.24 %8 Mar. %N 7 %T Two-step growth of HFCVD diamond films over large areas %@secondarytype PRE PI %K HFCVD, Diamond, Two-step growth, Large area. %@group %@group %@group LAS-CTE-INPE-MCT-BR %@group LAS-CTE-INPE-MCT-BR %@secondarykey INPE--PRE/ %@issn 0042-207X %2 sid.inpe.br/mtc-m18@80/2009/07.02.19.28.09 %@affiliation %@affiliation %@affiliation Instituto Nacional de Pesquisas Espaciais (INPE) %@affiliation Instituto Nacional de Pesquisas Espaciais (INPE) %P 1054-1056 %4 sid.inpe.br/mtc-m18@80/2009/07.02.19.28 %D 2009 %V 89 %@doi 10.1016/j.vacuum.2008.11.013 %A Amorim, A., %A Nascente, P. A. P., %A Trava-Airoldi, Vladimir Jesus, %A Corat, Evaldo José, %A Alves, A. R., %A Moro, J. R., %@dissemination WEBSCI; PORTALCAPES; COMPENDEX. %@area FISMAT